Laboratory Work on Organic Chemistry (undergraduate specialty) class introduction course

主题目录

• 常规

  全部折叠 展开全部
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    Japanese 网页地址
  • This page provides an easy-to-read overview of the class and relevant links.
    

    For the most up-to-date "Class Plan", "Grading Criteria and Methods," and other information,

    be sure to check the official syllabus of Hokkaido University.

    
    

  • Teacher

    • ANDO Yasuhiro (Faculty of Fisheries Sciences)
    • FUJITA Masaki (Faculty of Fisheries Sciences)  

• Summary of Laboratory Work on Organic Chemistry

  　The fundamentals of organic chemistry, from research on natural products of biological origin to organic synthesis, are reaction, purification, and identification. In addition, physiological functions of organic compounds are also important in the fields of aquatic chemistry and food chemistry. In living organisms, even slight structural changes can lead to major changes in biological activity, so rigorous purification and identification are extremely important techniques for understanding the functions of compounds. Therefore, in this experiment, lipids are mainly used as materials, and the objective is to acquire the following basic techniques and knowledge.

  ①　Acquire knowledge of basic techniques in handling organic compounds, their principles, and organic reactions.

  ②　Acquire knowledge and skills in the extraction and purification of natural organic compounds.

  ③　Acquire knowledge and skills in the analysis and identification of organic compounds by equipment.

  ④　Know the physiological functions of organic compounds by testing their bioactivity.

  
  

  　The main focus of this experiment is to actually work with one's own hands. Therefore, to the extent possible, this experiment was conducted by individuals rather than by groups.

• Basic Organic Reaction Operations
  • This is the basic flow of organic reaction operations

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• Basic operation of thin-layer chromatography (TLC)
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    Explanatory video of TLC 网页地址

• Basic operation of column chromatography
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    Explanatory video silica gel column chromatography 文件

    368.7 MB Video file (MP4) 上传 2023年04月27日 13:43

• Part 1: Ester hydrolysis
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    Explanatory video of ester hydrolysis 文件

    586.2 MB Video file (MP4) 上传 2023年04月27日 13:43

• Part 2: Esterification of carboxylic acids
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    Explanatory video of esterification of carboxylic acids 文件

    365.3 MB Video file (MP4) 上传 2023年04月27日 13:43

• Part 3: Hydrogen bromide addition to double bonds
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    Explanatory video of hydrogen bromide addition to double bonds 文件

    284.7 MB Video file (MP4) 上传 2023年04月27日 13:43

• Part 4: Elimination of hydrogen bromide
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    Explanatory video of elimination of hydrogen bromide 文件

    352.2 MB Video file (MP4) 上传 2023年04月27日 13:43

• Part 5: Reduction of esters to alcohols
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    Explanatory video of reduction of esters to alcohols 文件

    360.6 MB Video file (MP4) 上传 2023年04月27日 13:43

• Part 6: Derivatization and bioassay of alcohols
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    Explanatory video of derivatization and bioassay of alcohols 文件

    379.3 MB Video file (MP4) 上传 2023年04月27日 13:43

• Part 7: Extraction and quantification of vanillin from vanilla beans
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    Explanatory video of extraction and quantification of vanillin from 文件

    151.7 MB Video file (MP4) 上传 2023年04月27日 13:43

• Part 8: Synthesis and purification of vanillin
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    Explanatory video of synthesis and purification of vanillin 文件

    345.9 MB Video file (MP4) 上传 2023年04月27日 13:43

• LCMS basic operation
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    Explanatory video of LCMS sample preparation method 文件

    189.7 MB Video file (MP4) 上传 2023年04月27日 13:43

• NMR basic operation
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    Explanatory video of NMR sample preparation method 文件

    116.7 MB Video file (MP4) 上传 2023年04月27日 13:43

• 【Related Summary Course】